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LECTURE SCHEDULE |
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LECTURE SCHEDULE |
| 1 | Sep. 3 | Course Structure. Introduction | |
| 2 | Sep. 8 | Classification. Separative transport and selectivity. (Presentation topics to select.) | |
| 3 | Sep. 10 | GC Introduction. Adsorption and Partition GC. Capillary Columns. | |
| 4 | Sep. 15 | GC Theory | |
| 5 | Sep. 17 | GC Theory and Instrumentation | |
| 6 | Sep. 22 | GC Detectors. GC-MS, Interfaces, ionization (EI, CI) | |
| 7 | Sep. 24 | GC/MS (Mass-spec interpretation) | |
| 8 | Sep. 29 | SFC (Theory, Instrumentation, Applications) Purge&Trap, Thermal Desorption. (Presentation assignments). |
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| 9 | Oct. 1 | Head-Space analysis Frank Grande "GC Head-Space" Diego Alomonte "Chromatographic analysis of volatile sulfur compounds in wines using static head-space technique" |
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| 10 | Oct. 6 | Puar Tejinder "GC Separation of Fatty acids" Midterm exam. (take home) | |
| 11 | Oct. 8 | HPLC Introduction | |
| 12 | Oct. 13 | HPLC Instrumentation. Adsorbents, surface chemistry, types of stationary phases | |
| 13 | Oct. 15 | HPLC Theory. | |
| 14 | Oct. 20 | Spencer Maria "Particle
size separation" Efficiency (Effect of particle size, shape, particle size distribution). |
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| 15 | Oct. 22 | Bobrow, Lauren
"Column packing for LC" Rao Sabitha "Comparison between different stationary phases of RP HPLC" |
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| 16 | Oct. 27 | HPLC columns, Column selection, surface modification, column packing, column troubleshooting . | |
| 17 | Oct. 29 | Mellace Alfredo "Chiral
separation using cellulose stationary phase in LC" Yeung Leih-Shan "A systematic development of a method for sodium sufacetamide analysis." |
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| 18 | Nov. 3 | Galanti Michelle
"Discussion of method development of vecuronium bromide assy transfer from NP to RP
method" Shelton Christipher (TBA) |
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| 19 | Nov. 5 | HPLC retention, pH and solvent effect | |
| 20 | Nov.10 | HPLC Detectors | |
| 21 | Nov.12 | Size Exclusion HPLC, Ion-exchange, Ion-pair | |
| 22 | Nov.17 | Student presentation (TBA) | |
| 23 | Nov.19 | Student presentation (TBA) | |
| 24 | Nov.24 | LC/MS (Interfaces, Ionization principles) | |
| 25 | Nov.26 | Thanksgiving Recess | |
| 26 | Dec. 1 | Quantitative analysis, internal & external standards, method detection limit. | |
| 27 | Dec. 3 | CZE, Capillary electrochromatography | |
| 28 | Dec. 8 | Other separation modes (FFF, Membrane, Extraction) | |
| 29 | Dec.10 | Course overview. Final exam preparation | |
| 30 | Dec.15 | Final Exam. | |
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