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Chemistry 6205 |
Lecture Schedule | Spring 2006 |
| 1 | Jan. 12 | Course Structure. Introduction. Classification. Separative transport and selectivity, GC |
| 2 | Jan. 19 | Capillary Columns, Instrumentation, Sample introduction, GC Detectors. Adsorption and Partition in GC, GC Theory, Mass-transport theory |
| 3 | Jan. 26 | GC-MS, Interfaces, ionization (EI, CI), Mass-spec interpretation, SFC (Theory, Instrumentation, Applications), Purge&Trap, Thermal Desorption, Head-Space |
| 4 | Feb. 2 | HPLC Introduction, HPLC Instrumentation, HPLC Detectors |
| 5 | Feb. 9 | Adsorbents, surface chemistry, types of
stationary phases, HPLC columns, Column selection, surface modification, column packing, column troubleshooting (Midterm take-home) |
| 6 | Feb. 16 | HPLC Theory, Retention Mechanism, (Midterm due) |
| 7 | Feb. 23 | pH and solvent effect, pH and pKa shift, Chaotropic effect |
| 8 | Mar. 2 | Size Exclusion HPLC, Ion-exchange, Ion-pair, CZE/CEC |
| 9 | Mar. 16 | LC/MS (Interfaces, principles, Applications) |
| 10 | Mar. 23 | CZE, CEC (electrodriven separations) |
| 11 | Mar. 30 | Presentations I |
| 12 | Apr. 6 | Presentations II |
| 13 | Apr. 20 | Presentations III |
| 14 | Apr. 27 | Wrap up (overview of the course) Take home final. |
| 15 | ? | Final exam |
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All links in the Lecture Schedule are given to the navigation page of the book. Select your topic from the pop-up list on the left.
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